Petrochemical

Real-time VOC analysis for petrochemical applications that speeds up time to data in oil & gas surveying and production. Increase your capacity and shorten lead times in hydrocarbon characterization, BTEX fenceline monitoring, sour gas detection, and mudlogging.

The selective, sensitive, rapid, and robust analysis provided by SIFT-MS makes it uniquely suited to outdoor air quality monitoring.  SIFT-MS enables potential environmental incidents to be detected, identified, and remedied quickly, before they escalate to social or regulatory issues.

This webinar describes continuous environmental monitoring applications and presents a variety of case studies, including:

• Fenceline monitoring
• Real-time stack gas analysis
• Odor characterization at the source
• Continuous odor monitoring

We present the results of the first study where SIFT-MS was used to detect and quantify hydrogen sulfide in natural gas and liquefied petroleum gas (LPG).  SIFT-MS very effectively detects and quantifies hydrogen sulfide to mid part-per-billion levels in natural gas and LPG (due to the need for dilution).  The degree of souring of natural gas, in addition to determining its light to medium hydrocarbon composition, can be determined.

SIFT-MS presents a breakthrough in the detection, quantitation and tracing of petroleum hydrocarbons.  This brochure outlines several SIFT-MS-based petrochemical industry solutions provided by Syft Technologies including mud logging, sour gas detection, oil and gas prospecting, leak detection, and fence line monitoring.

The sensitivity, selectivity, and high-speed analysis provided by SIFT-MS provides fast, reliable, and economic analysis of drilling mud at the well site.  Learn more about how it provides comprehensive, quantitative C1 – C14 analysis of mud gas in less than 15 seconds to part-per-billion-by volume concentrations (ppbv).

The combination of SIFT-MS and a GERSTEL autosampler provides automated analysis of benzene, toluene, ethylbenzene and the xylenes (BTEX) sampled from ambient air using thermal desorption tubes. This application note demonstrates the repeatability and sensitivity possible with automated thermal desorption (TD)-SIFT-MS. Automated TD-SIFT-MS provides sample throughput >3 three-fold higher than conventional TD-gas chromatography methods.

Selected ion flow tube mass spectrometry (SIFT-MS) combined with GERSTEL automation greatly simplifies analysis of benzene, toluene, ethylbenzene and the xylenes (BTEX) in water. This application note demonstrates the linearity, repeatability and sensitivity achievable with automated SIFT-MS. Automated static headspace (SH)-SIFT-MS provides sample throughputs at least three-fold higher than traditional purge-and-trap-gas chromatography methods.

Combining direct analysis using selected ion flow tube mass spectrometry (SIFT-MS) and automated sample preparation, determination of benzene, toluene, ethylbenzene, and the xylenes (BTEX) in soil via methanolic extraction is simplified and accelerated. This application note provides an initial validation of the automated SIFT-MS method and demonstrates that the sample throughput achievable with SIFT-MS is at least two-fold higher than gas chromatography (GC).

In this webinar, we describe various automotive applications of SIFT-MS including exhaust gas analysis, emission screening of synthetic and natural vehicle components, and leak detection. Implementations of SIFT-MS instrumentation range from R&D through to the process line, enabling timely decisions to be made from new product development right through to production.

In this webinar, we describe applications of SIFT-MS to diverse process and specialty gas applications.  The strength of SIFT-MS lies in the combination of four factors that other techniques lack:

• Rapid analysis
• Comprehensive compound detection, including highly reactive species
• Selectivity
• Simple, low-cost operation

SIFT-MS is an instrument for achieving real-time, selective and economical trace analysis of contaminants in hydrogen fuel. Direct, broad-spectrum analysis using SIFT-MS provides unique capabilities in hydrogen transport applications, including:

• Simple NH3, CH2O, CHOOH analysis
• Monitoring of real time oxidation of 13CO into 13CO2
• Real time monitoring of contaminant degradation in fuel cell stacks.

It has been historically impossible to monitor real-time oxidation of CO into CO2 onto the PEM fuel cell surface due to technical complexity.  The UK National Physical Laboratory (NPL) developed an approach using 13 CO contaminated hydrogen to monitor real-time 13 CO2 and 12 CO2 by SIFT-MS negative reagent ions. This presentation highlights the NPL setup, the calibration of the measurement in humidified atmosphere, and the first isotopic measurements for fuel cell research.

In this first-of-its-kind presentation, Dr. Thomas Bacquart describes his research at the UK National Physical Laboratory: development of new measurement standards for hydrogen fuel purity.  Dr. Bacquart presents his SIFT-MS results, which include determination of reactive, chromatographically challenging impurities such as ammonia, formaldehyde and hydrogen sulfide.

SIFT-MS represents a breakthrough in the detection and quantitation of VOCs (such as benzene and formaldehyde) and inorganic gases (such as sulfur dioxide and hydrogen sulfide).  This webinar presents a variety of SIFT-MS-based petrochemical industry applications, including:

• Mud logging
• Stack analysis
• Fenceline monitoring
• Process analysis (e.g. for catalysis research)
• Polymer product quality control and assurance

Become acquainted with TD-SIFT-MS through the analysis of environmental BTEX (benzene, toluene, ethylbenzene and xylene) from multiple sorbent tubes. This demonstration will address the following; - What makes this approach unique? - What does “real-time” thermal desorption data look like? - How is the automation and processing software operated? - How fast is it?

Mark describes how the ICH Q 2 (R1) guidelines can be readily applied to SIFT-MS methods, whether in scenarios where only the analytical technique is changed or for tasks that pose a unique analytical challenge. He presents case studies for two such scenarios: 1) methanolic extraction of BTEX compounds (benzene, toluene, ethylbenzene plus xylenes) from soil, 2) direct analysis of formaldehyde leaching into single-use pharmaceutical devices from polymeric components.

This app note introduces the next generation of SIFT-MS, Syft Tracer^TM, which launched at Pittcon 2023.  It revolutionizes volatile impurities analysis workflows through unparalleled speed, performance stability, and reproducibility.  Learn about how this innovation to real-time trace gas detection outpaces chromatography-based methods in the analysis of challenging analytes such as formaldehyde in a PEG excipient.

Join us for this webinar to learn about Syft Tracer, the latest advancement of real-time, trace gas analysis by SIFT-MS which launched at Pittcon 2023. Hear how the recent product innovations unlock analytical bottlenecks and enable faster decisions to be made in critical process steps.

Syft Tracer^TM is the latest advancement in real-time, direct injection mass spectrometry (MS) built to solve the most difficult analytical challenges faced within a variety of industries and applications.  This advancement to SIFT-MS delivers trace-level detection sensitivity, unparalleled performance stability, superior selectivity, and highly reproducible, quantitative data.  Syft Tracer is optimized for high-throughput environments where continuous operation is the standard.  Never miss a product or environmental contamination event again.

This application note describes a scenario in which Syft Tracer^TM replaces five chromatography systems and still has significant available sample capacity. SIFT-MS provides rapid, chromatography-free analysis that revolutionizes multiple workflows.

This study demonstrates high-throughput analysis of BTEX compounds from several matrices (air, water and soil). Detection limits in the single-digit part-per-billion concentration range (by volume) are readily achievable within seconds using SIFT-MS, because sample analysis is achieved without chromatography, pre-concentration, or drying.  We also present a calibration approach that enables speciation of ethylbenzene from the xylenes in real time.

The characteristic flexibility, stability, high throughput, and fast time to data of the Syft Tracer next-gen SIFT-MS instrument apply across multiple headspace approaches for diverse matrices. This application note briefly summarizes the use of (1) dissolution, (2) multiple headspace extraction (MHE), and (3) the method of standard additions, then provides a guide for identifying the appropriate headspace approach for various matrices.

This application note investigates concentration dependence of MHE calibration in sample matrix.  Across the full range of analytes investigated in this study, MHE calibration holds for at least one order of magnitude change in sample concentration.  For analytes in the C7–C9 range, the MHE calibration applies over two orders of magnitude analyte concentration. These results mean that the MHE workflow can be applied to a wider range of samples in the matrix, further reducing calibration demand.